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An Asymmetric Synthesis of a Chiral Sulfone Acid with Concomitant Hydrolysis and Oxidation to Enable the Preparation of a Glucokinase Activator

JOURNAL ARTICLE published 21 September 2012 in Organic Process Research & Development

Authors: Amy C. DeBaillie | Nicholas A. Magnus | Michael E. Laurila | James P. Wepsiec | J. Craig Ruble | Jeffrey J. Petkus | Radhe K. Vaid | Jeffry K. Niemeier | Joseph F. Mick | Thomas Z. Gunter

https://doi.org/10.1021/op300139g Actions

A Practical Synthesis of the PDE4 Inhibitor, KW-4490

JOURNAL ARTICLE published 17 September 2010 in Organic Process Research & Development

Authors: Arata Yanagisawa | Koichiro Nishimura | Kyoji Ando | Tetsuya Nezu | Ayako Maki | Sachiko Kato | Wakako Tamaki | Eiichiro Imai | Shin-ichiro Mohri

https://doi.org/10.1021/op1001287 Actions

A New and Improved Process for Celiprolol Hydrochloride

JOURNAL ARTICLE published 1 March 2001 in Organic Process Research & Development

Authors: Ramesh A. Joshi | Mukund K. Gurjar | Narendra K. Tripathy | Mukund S. Chorghade

https://doi.org/10.1021/op000297l Actions

A Practical Synthesis of Enantiopure 7-Alkoxy-4-aryl-tetrahydroisoquinoline, a Dual Serotonin Reuptake Inhibitor/Histamine H3 Antagonist

JOURNAL ARTICLE published 1 November 2007 in Organic Process Research & Development

Authors: Xiaohu Deng | Jimmy T. Liang | Jing Liu | Heather McAllister | Carsten Schubert | Neelakandha S. Mani

https://doi.org/10.1021/op700183q Actions

Practical Synthesis of an Orally Active CCR5 Antagonist, 7-{4-[2-(Butoxy)- ethoxy]phenyl}-N-(4-{[methyl(tetrahydro-2H-pyran-4-yl)amino]methyl}phenyl)- 1-propyl-2,3-dihydro-1H-1-benzazepine-4-carboxamide

JOURNAL ARTICLE published 1 March 2005 in Organic Process Research & Development

Authors: Tomomi Ikemoto | Tatsuya Ito | Atsuko Nishiguchi | Syotaro Miura | Kiminori Tomimatsu

https://doi.org/10.1021/op0497916 Actions

The Large-Scale Synthesis of (S)-N-Boc-bis(4-fluorophenyl)alanine

JOURNAL ARTICLE published 18 January 2013 in Organic Process Research & Development

Authors: Robert B. Appell | Lee T. Boulton | Edward D. Daugs | Matt Hansen | Christopher H. Hanson | Jerry Heinrich | Christel Kronig | Richard C. Lloyd | David Louks | Mark Nitz | Céline Praquin | James A Ramsden | Helen Samuel | Mark Smit | Matthew Willets

https://doi.org/10.1021/op3002855 Actions

First Scale-Up: Problems and Resolutions on the Synthesis of WAY-253752, a Novel, Dual-Acting SSRI/5HT1A Antagonist

JOURNAL ARTICLE published 1 January 2008 in Organic Process Research & Development

Authors: Antonia Nikitenko | Deborah Evrard | Annmarie L. Sabb | Robert L. Vogel | Gary Stack | Mairead Young | Melissa Lin | Boyd L. Harrison | John R. Potoski

https://doi.org/10.1021/op700181n Actions

Sustainability and Biotechnology

JOURNAL ARTICLE published 21 January 2011 in Organic Process Research & Development

Authors: Hans-Peter Meyer

https://doi.org/10.1021/op100206p Actions

Kinetic Study of Addition of Some Carboxylic Acids to 1,2-Epoxy-3-phenoxypropane

JOURNAL ARTICLE published 1 November 1999 in Organic Process Research & Development

Authors: Agnieszka Bukowska | Wiktor Bukowski

https://doi.org/10.1021/op9900479 Actions

Facile Production Scale Synthesis of (S)-Taniguchi Lactone: A Precious Building-Block

JOURNAL ARTICLE published 16 May 2014 in Organic Process Research & Development

Authors: Fredrik von Kieseritzky | Yeliu Wang | Magnus Axelson

https://doi.org/10.1021/op500096j Actions

Efficient Multikilogram Synthesis of a VLA-4 Antagonist via a Povarov Reaction

JOURNAL ARTICLE published 15 May 2020 in Organic Process Research & Development

Authors: Patrick Cerfontaine | Frank Driessens | Marie-France Deltent | Sylvain Petit

https://doi.org/10.1021/acs.oprd.9b00421 Actions

Process Development and Scale-Up of AZD7545, a PDK Inhibitor

JOURNAL ARTICLE published 16 March 2012 in Organic Process Research & Development

Authors: Bharti Patel | Catherine R. Firkin | Evan W. Snape | Shelley L. Jenkin | David Brown | Julian G. K. Chaffey | Philip A. Hopes | Carl D. Reens | Mike Butters | Jonathan D. Moseley

https://doi.org/10.1021/op2003419 Actions

Synthetic Route Discovery and Introductory Optimization of a Novel Process to Idebenone

JOURNAL ARTICLE published 20 May 2011 in Organic Process Research & Development

Authors: Anna Tsoukala | Hans-René Bjørsvik

https://doi.org/10.1021/op200051v Actions

The Impact of Process Chemists and Engineers on Green Chemistry

JOURNAL ARTICLE published 21 November 2008 in Organic Process Research & Development

Authors: NealG. Anderson

https://doi.org/10.1021/op800259p Actions

Stereoselective Lithiation and Carboxylation of Boc-Protected Bicyclopyrrolidine: Synthesis of a Key Building Block for HCV Protease Inhibitor Telaprevir

JOURNAL ARTICLE published 17 October 2014 in Organic Process Research & Development

Authors: Gerald J. Tanoury | Minzhang Chen | Yong Dong | Raymond Forslund | Valdas Jurkauskas | Andrew D. Jones | Daniel Belmont

https://doi.org/10.1021/op500040j Actions

Production of Hydrogen Peroxide via Aerobic Oxidation of Alcohols Catalyzed by N-Hydroxyphthalimide

JOURNAL ARTICLE published 1 March 2000 in Organic Process Research & Development

Authors: Takahiro Iwahama | Satoshi Sakaguchi | Yasutaka Ishii

https://doi.org/10.1021/op990082f Actions

Synthetic Process Development of BMS-599793 Including Azaindole Negishi Coupling on Kilogram Scale

JOURNAL ARTICLE published 21 June 2013 in Organic Process Research & Development

Authors: Stanislaw Pikul | Hua Cheng | Allen Cheng | C. D. Huang | Alex Ke | LungHuang Kuo | Andrew Thompson | Susan Wilder

https://doi.org/10.1021/op400012p Actions

Total Synthesis of Hematoporphyrin and Protoporphyrin: A Conceptually New Approach

JOURNAL ARTICLE published 16 July 2010 in Organic Process Research & Development

Authors: Pierre Martin | Markus Mueller | Dietmar Flubacher | Andreas Boudier | Hans-Ulrich Blaser | Dirk Spielvogel

https://doi.org/10.1021/op100036c Actions

Scale-Up of a Continuous Extraction Process for Driving an Equilibrium-Limited Reaction to Completion

JOURNAL ARTICLE published 16 November 2018 in Organic Process Research & Development

Authors: Michael T. Tudesco | Eric G. Moschetta | Eric A. Voight

https://doi.org/10.1021/acs.oprd.8b00260 Actions

Improved Synthesis of 6-Chloro-5-methylpyridin-2-amine: A Key Intermediate for Making Lumacaftor

JOURNAL ARTICLE published 19 June 2020 in Organic Process Research & Development

Research funded by Chinese Academy of Sciences (XDA12040327,XDA12050411)

Authors: Junchi Zhang | Fuqiang Zhu | Guanghui Tian | Xiangrui Jiang | Jingshan Shen

https://doi.org/10.1021/acs.oprd.9b00556 Actions
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